| 英文名 | 4-Bromobenzoyl acetonitrile |
|---|---|
| 类型 | 芳香族化合物 |
| CAS号 | 4592-94-3 |
| 物理性质 | M 224.1, m 160-164℃, 162.4-163.4℃. |
| 提纯方法 | The nitrile is purified by dissolving in slightly alkaline H2O (charcoal), filtering and acidifying with HCl to give colourless needles (m 162-163℃). It recrystallises from EtOH. With Me2SO4/KOH at 130℃ it gives 4-bromo ?? - methoxycinnamylnitrile m 58.5-59.5℃(from high boiling pet ether) [Fuson & Wolf J Am Chem Soc 61 1940 1939, Grathaus & Dains J Am Chem Soc 58 1334 1936]. [Beilstein 10 III 2998.] |
| 相关文献 | 暂无权限 |
扩展信息
