| 英文名 | 3-Indoleacetonitrile |
|---|---|
| 类型 | 杂环化合物 |
| CAS号 | 771-51-7 |
| 物理性质 | M 156.2, m 33-36℃, 36-38℃, b 157℃/0.2mm, 158-160℃/0.1mm, viscous oil nD20 1.6097. |
| 提纯方法 | Distil the nitrile at very high vacuum, and the viscous distillate crystallises on standing after a few days; the picrate has m 127-128℃(from EtOH) [Coker et al. J Org Chem 2 7 850 1962, Thesing & Schülde Chem Ber 85 324 1952]. Store it away from light. The N-acetate has m 118℃(from MeOH) and has RF= 0.8, on Silica Gel F 254 in CHCl2 /MeOH 19:1 [Buzas et al. Synthesis 129 1977]. [Beilstein 22 III/IV 1097, 22/3 V 74.] |
| 相关文献 | 暂无权限 |
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