英文名 | 2-Acetamidofluorene |
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英文别名 | N-(2-fluorenyl)acetamide |
类型 | 芳香族化合物 |
CAS号 | 53-96-3 |
物理性质 | M 223.3, m 194℃, 196-198℃. |
提纯方法 | Recrystallise it from toluene (1.3mg in 100mL). Its solubility in H2O is 1.3mg/L at 25℃, UV: λ max nm(log ) : 288(4.43), 313(4.13). [Sawicki J Org Chem 21 271 1956.] It can also be recrystallised from 50% AcOH. [Diels et al. Chem Ber 35 3285 1902]. 9-14 C and - 14 C 2-acetamidofluorene were recrystallised from aqueous EtOH and had m 194-195℃and 194℃respectively. [Miller et al. Cancer Res 9 504 1949, 10 616 1950, Sadin et al. J Am Chem Soc 74 5073 1952, Beilstein 12 H 3287, 12 IV 3373.] |
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