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英文名 Formaldehyde dimethyl acetal
英文别名 dimethoxymethane, methylal, formal
类型 脂肪族化合物
CAS号 109-87-5
物理性质 M 76.1, m -108℃, b 41-42℃/736mm, 41-43℃/atm, 42-46℃/atm, d420 0.8608, nD20 1.35335.
提纯方法 It is a volatile flammable liquid which is soluble in three parts of H2O, and is readily hydrolysed by acids. Purify it by shaking with an equal volume of 20% aqueous NaOH, stand for 20minutes, dry over fused CaCl2, filter and fractionally distil it through an efficient column. Store it over molecular sieves. [Buchler et al. Org Synth Coll Vol III 469 1955, Rambaud & Besserre Bull Soc Chim Fr 45 1955, IR: Wilmshurst Can J Chem 36 285 1958, Beilstein 1 IV 3026.]
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数据更新时间:2025-04-21

Formaldehyde dimethyl acetal提纯方法

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